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ASTM D7214-07a(2012)..
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ASTM D3244-12
Standard Practice for Utilization of Test Data to Determine Conformance with Specifications
STANDARD published on 1.12.2012
The information about the standard:
Designation standards: ASTM D3244-12
Note: WITHDRAWN
Publication date standards: 1.12.2012
SKU: NS-23008
The number of pages: 11
Approximate weight : 33 g (0.07 lbs)
Country: American technical standard
Category: Technical standards ASTM
The category - similar standards:
Annotation of standard text ASTM D3244-12 :
Keywords:
acceptance, acceptance limits, agreement, conformance, dispute, precision, rejection, specifications, ICS Number Code 75.100 (Lubricants, industrial oils and related products)
Additional information
| Significance and Use | ||||||||||||||||||
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4.1 This practice provides a means whereby the parties to a transaction can resolve potential quality disputes over those product properties which can be tested and expressed numerically. 4.1.1 This practice can be used to ensure that such properties are correctly stated on labels or in other descriptions of the product. 4.1.2 This practice can be implemented in those cases where a supplier uses an in-house or a commercial testing laboratory to sample and test a product prior to releasing the product to a shipper (intermediate receiver) and the ultimate receiver also uses an in-house or commercial testing laboratory to sample and test the product upon arrival at the destination. The ATV would still be determined according to 8.3. 4.2 This practice can assist in the determination of tolerances from specification limits which will ensure that the true value of a property is sufficiently close to the specification value with a mutually agreed probability so that the product is acceptable to the receiver. Such tolerances are bounded by an acceptance limit (AL). If the ATV value determined by applying this practice falls on the AL or on the acceptable side of the AL, the product can be accepted; otherwise it shall be deemed to have failed the product acceptance requirement established by applying this practice. 4.3 Application of this practice requires the AL be determined prior to actual commencement of testing. Therefore, the degree of criticality of the specification, as determined by the Probability of Acceptance (P value) that is required to calculate the 4.3.1 This agreement should include a decision as to whether the ATV is to be determined by the absolute or rounding-off method of Practice E29, as therein defined. 4.3.1.1 If the rounding-off method is to be used, the number of significant digits to be retained must also be agreed upon. 4.3.1.2 These decisions must also be made in the case where only one party is involved, as in the case of a label. 4.3.1.3 In the absence of such an agreement, this practice recommends the ATV be rounded in accordance with the rounding-off method in Practice E29 to the number of significant digits that are specified in the governing specification. 4.4 This practice is designed to be suitable for reference in contracts governing the transfer of petroleum products and lubricants from a supplier to a receiver. 4.5 As a prerequisite for acceptance for lab test results to be used in this practice, the following conditions shall be satisfied: 4.5.1 Site precision (R′) as defined in Practice D6299 for the appropriate test method(s) from each lab, as substantiated by in-house quality control programs, for property typical of the product in dispute, should have a TPI > 1.2 (see Practice D6792 for TPI explanation), but at a minimum shall be better than the published method reproducibility (R). 4.5.2 Each lab shall be able to demonstrate, by way of results from interlaboratory exchange programs, a lack of a systemic bias relative to exchange averages for the appropriate test method(s) as per methodology outlined in Guide D7372. 4.5.3 In the event that the site precision of laboratories from two parties are statistically different as confirmed by the F-test (see Annex A4), then, for the purpose of establishing the ATV, each laboratory's test result shall be inversely weighted in accordance with laboratory's demonstrated variance. 4.6 It is recommended that this practice be conducted under the guidance of a qualified statistician. |
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| 1. Scope | ||||||||||||||||||
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1.1 This practice covers guidelines and statistical methodologies with which two parties, usually a supplier and a receiver, can compare and combine independently obtained test results to obtain an Assigned Test Value (1.2 This practice defines a technique for comparing an ATV with a specification limit. 1.3 This practice applies only to those test methods which specifically state that the repeatability and reproducibility values conform to the definitions herein. 1.4 The statistical principles and
methodology outlined in this practice can also be used to obtain an
Standard Test Method for Hydrocarbon
Types in Liquid Petroleum Products by Fluorescent Indicator
Adsorption (Includes all amendments and changes 9/14/2020). Standard Guide for Analysis and
Interpretation of Proficiency Test Program Results Standard Practice for Manual Sampling of
Petroleum and Petroleum Products Standard Practice for Automatic Sampling
of Petroleum and Petroleum Products (Includes all amendments and
changes 3/24/2023). Standard Practice for Applying
Statistical Quality Assurance and Control Charting Techniques to
Evaluate Analytical Measurement System Performance (Includes all
amendments and changes 12/12/2023). Standard Practice for Determination of
Precision and Bias Data for Use in Test Methods for Petroleum
Products, Liquid Fuels, and Lubricants Standard Practice for Quality Management
Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing
Laboratories (Includes all amendments and changes 12/7/2023). Standard Practice for Using Significant
Digits in Test Data to Determine Conformance with
Specifications ISO 4259 Determination and Application of
Precision Data in Relation to Methods of Test |
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