ASTM D7861-14(2019)

Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy

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STANDARD published on 1.5.2019

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The information about the standard:

Designation standards: ASTM D7861-14(2019)
Note: WITHDRAWN
Publication date standards: 1.5.2019
SKU: NS-953507
The number of pages: 7
Approximate weight : 21 g (0.05 lbs)
Country: American technical standard
Category: Technical standards ASTM

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Liquid fuels

Annotation of standard text ASTM D7861-14(2019) :

Keywords:

biodiesel, biodiesel blend, biodiesel concentration, FAME, fatty acid methyl esters, infrared spectroscopy,, ICS Number Code 75.160.20 (Liquid fuels)

Additional information

Significance and Use

5.1 Biodiesel is a fuel commodity primarily used as a blending component with diesel fuel. It is important to check the concentration of biodiesel in the diesel fuel in order to make sure it is either not below the minimum allowable limit and or does not exceed the maximum allowable limit.

5.2 This test method is applicable for quality control in the production and distribution of diesel fuel and biodiesel blends.

1. Scope

1.1 This test method determines fatty acid methyl esters (FAME or biodiesel) in diesel fuel oils. FAME can be quantitatively determined from 1.0 % to 30.0 % by volume. This test method uses linear variable filter (LVF) array based mid-infrared spectroscopy for monitoring FAME concentration.

Note 1: See Section 6 for a list of interferences that could affect the results produced from this method.

1.2 This test method uses a horizontal attenuated total reflectance (HATR) crystal and a univariate calibration.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

2. Referenced Documents

D1298-12b(2017)e1	Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method (Includes all amendments and changes 3/14/2023).
D4052-22	Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D4057-22	Standard Practice for Manual Sampling of Petroleum and Petroleum Products
D4177-22e1	Standard Practice for Automatic Sampling of Petroleum and Petroleum Products (Includes all amendments and changes 3/24/2023).
D4307-17(2021)	Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
D975-23a	Standard Specification for Diesel Fuel (Includes all amendments and changes 12/19/2023).
D6299-23a	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (Includes all amendments and changes 12/12/2023).
D6300-24	Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
D6751-23a	Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels (Includes all amendments and changes 5/3/2023).
D7371-14(2022)	Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
D5854-19a	Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products (Includes all amendments and changes 8/13/2019).
E1655-17	Standard Practices for Infrared Multivariate Quantitative Analysis
E168-16(2023)	Standard Practices for General Techniques of Infrared Quantitative Analysis
D7467-23	Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)

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