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ASTM E352-13

Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

STANDARD published on 1.2.2013

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The information about the standard:

Designation standards: ASTM E352-13
Note: WITHDRAWN
Publication date standards: 1.2.2013
SKU: NS-46525
The number of pages: 36
Approximate weight : 108 g (0.24 lbs)
Country: American technical standard
Category: Technical standards ASTM

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The category - similar standards:

Chemical analysis of metals

Annotation of standard text ASTM E352-13 :

Keywords:

atomic absorption, chromium, cobalt, combustion analysis, copper, gravimetric, high-alloy steel, induction furnace, infrared absorption, ion exchange, lead, nickel, manganese, molybdenum, phosphorus, silicon, spectrophotometric, sulfur, tin, titration, titrimetric, tool steels, total carbon, vanadium, ICS Number Code 77.040.30 (Chemical analysis of metals)

Additional information

Significance and Use

4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications particularly those under the jurisdiction of ASTM Committee A1 on Steel, Stainless Steel, and Related Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.

1. Scope

1.1 These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

Element

Composition Range, %

Aluminum

0.005 to 1.5

Boron

0.001 to 0.10

Carbon

0.03 to 2.50

Chromium

0.10 to 14.0

Cobalt

0.10 to 14.0

Copper

0.01 to 2.0

Lead

0.001 to 0.01

Manganese

0.10 to 15.00

Molybdenum

0.01 to 10.00

Nickel

0.02 to 4.00

Nitrogen

0.001 to 0.20

Phosphorus

0.002 to 0.05

Silicon

0.10 to 2.50

Sulfur

0.002 to 0.40

Tungsten

0.01 to 21.00

Vanadium

0.02 to 5.50

1.2 The test methods in this standard are contained in the sections indicated below:

Sections

Carbon, Total, by the Combustion—
Thermal Conductivity Method—

Carbon, Total, by the Combustion Gravimetrical
Method—Discontinued

Chromium by the Atomic Absorption Method

(0.006 % to 1.00 %)

174

Chromium by the Peroxydisulfate
Oxidation—Titration Method

(0.10 % to 14.00 %)

184

Chromium by the Peroxydisulfate-Oxidation
Titrimetric Method—Discontinued 1980

Cobalt by the Ion-Exchange—
Potentiometric Titration Method

(2 % to 14 %)

Cobalt by the Nitroso-R-Salt
Spectrophotometric Method

(0.10 % to 5.0 %)

Copper by the Neocuproine
Spectrophotometric Method

(0.01 % to 2.00 %)

Copper by the Sulfide Precipitation-
Electrodeposition Gravimetric Method

(0.01 % to 2.0 %)

Lead by the Ion-Exchange—Atomic
Absorption Method

(0.001 % to 0.01 %)

Nickel by the Dimethylglyoxime
Gravimetric Method

(0.1 % to 4.0 %)

144

Manganese by the Periodate
Spectrophotometric Method

(0.10 % to 5.00 %)

Molybdenum by the Ion Exchange–
8-Hydroxyquinoline Gravimetric Method

203

Molybdenum by the Spectrophotometric Method

(0.01 % to 1.50 %)

162

Phosphorus by the Alkalimetric Method

(0.01 % to 0.05 %)

136

Phosphorus by the Molybdenum Blue
Spectrophotometric Method

(0.002 % to 0.05 %)

Silicon by the Gravimetric Method

(0.10 % to 2.50 %)

Sulfur by the Gravimetric
Method—Discontinued 1988

Sulfur by the Combustion-Iodate
Titration Method—Discontinued

Sulfur by the Chromatographic
Gravimetric Method—Discontinued 1980

Tin by the Solvent Extraction—
Atomic Absorption Method

(0.002 % to 0.10 %)

152

Vanadium by the Atomic
Absorption Method

(0.006 % to 0.15 %)

193

1.3 Test methods for the determination of carbon and sulfur not included in this standard can be found in Test Methods E1019.

1.4 Some of the composition ranges given in 1.5 The values stated in SI units are to be regarded as standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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